Object[Protocol, CyclicVoltammetry]
A protocol to perform cyclic voltammetry measurements of the input samples, using an electrochemical reactor.
Organizational Information
Name
Name of this Object.
Format: Single
Class: String
Programmatic Pattern: _String
Pattern Description: A string.
ID
ID of this Object.
Format: Single
Class: String
Programmatic Pattern: _String
Pattern Description: The ID of this object.
Object
Object of this Object.
Format: Single
Class: Expression
Programmatic Pattern: Object[Protocol, CyclicVoltammetry, _String]
Pattern Description: The object reference of this object.
Type
Type of this Object.
Format: Single
Class: Expression
Programmatic Pattern: Object[Protocol, CyclicVoltammetry]
Pattern Description: Object[Protocol, CyclicVoltammetry]
Notebook
Notebook this object belongs to.
Format: Single
Class: Link
Programmatic Pattern: _Link
Pattern Description: An object of that matches ObjectP[Object[LaboratoryNotebook]].
Relation: Object[LaboratoryNotebook][Objects]
Author
The investigator who created this protocol.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[User][ProtocolsAuthored]
General
DateConfirmed
The date on which the protocol first entered processing or a backlog.
Format: Single
Class: Date
Programmatic Pattern: _?DateObjectQ
DateEnqueued
The date on which the protocol was accepted and added to the queue.
Format: Single
Class: Date
Programmatic Pattern: _?DateObjectQ
DateStarted
The date on which the protocol moved from the front of the queue to begin running in the lab.
Format: Single
Class: Date
Programmatic Pattern: _?DateObjectQ
DateCompleted
The date on which the last step of this protocol's execution was finished.
Format: Single
Class: Date
Programmatic Pattern: _?DateObjectQ
DateCanceled
The date on which the protocol was canceled and removed from the queue.
Format: Single
Class: Date
Programmatic Pattern: _?DateObjectQ
Script
The script that created this protocol.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Notebook][Protocols]
SubprotocolScripts
All scripts generated by this protocol as a list of subprotocols.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Notebook, Script][ParentProtocol]
Site
The ECL site at which this protocol was executed.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Container, Site]
SamplesIn
Input samples for this analytical or preparative experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
ContainersIn
Any containers containing this protocols' SamplesIn.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
NumberOfReplicates
Indicates the number of times the experiment is repeated with identical parameters.
Format: Single
Class: Integer
Programmatic Pattern: GreaterP[0, 1]
Status
The current status of the protocol.
Format: Single
Class: Expression
Programmatic Pattern: ProtocolStatusP
CheckpointProgress
A listing of all the checkpoints passed in the execution of this protocol.
Format: Multiple
[[1]] Name
Header: Name
Class: String
Programmatic Pattern: _String
[[2]] Start Time
Header: Start Time
Class: Date
Programmatic Pattern: _?DateObjectQ
[[3]] End Time
Header: End Time
Class: Date
Programmatic Pattern: _?DateObjectQ|Null
SubprotocolDescription
A short title indicating what this subprotocol accomplishes.
Format: Single
Class: String
Programmatic Pattern: _String
BatchedUnitOperations
The individual batches of the protocol, as they will be executed in the lab.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[UnitOperation][Protocol]
ReplacementProtocol
If this protocol was aborted due to technical reasons, links to the replacement protocol run in its place.
Format: Single
Class: Link
Programmatic Pattern: _Link
Sterile
Indicates if the protocol is performed in a sterile environment.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
LiquidHandlingLog
The instrumentation trace file that monitored and recorded the execution of this robotic liquid handling.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[EmeraldCloudFile]
PooledSamplesIn
The members of SamplesIn gathered into the pools that are mixed in each AliquotContainer.
Format: Multiple
Class: Expression
Programmatic Pattern: {ObjectReferenceP[Object[Sample]]..}
NestedIndexMatchingSamplesIn
The members of SamplesIn gathered into the pools that are mixed in each AliquotContainer.
Format: Multiple
Class: Expression
Programmatic Pattern: {ObjectReferenceP[Object[Sample]]..}
InitialNitrogenPressure
The pressure data of the nitrogen gas source before starting the experiment.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
NitrogenPressureLog
The pressure log for the nitrogen gas source for the relevant section of the facility.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
InitialCO2Pressure
The pressure data of the CO2 gas source before starting the experiment.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
CO2PressureLog
The pressure log for the CO2 gas source for the relevant section of the facility.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
InitialArgonPressure
The pressure data of the argon gas source before starting the experiment.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
HoldOrder
Indicates if the queue position of this protocol should be strictly enforced, regardless of the available resources in the lab.
Format: Single
Class: Boolean
Programmatic Pattern: BooleanP
Priority
Indicates if this protocol should be prioritized to start at the given StartDate, have dedicated operation for its entirety, and not be interrupted by other protocols.
Format: Single
Class: Boolean
Programmatic Pattern: BooleanP
StartDate
The date at which this protocol should be prioritized to start.
Format: Single
Class: Date
Programmatic Pattern: _?DateObjectQ
Branch
The git branch that this protocol should be run on.
Format: Single
Class: String
Programmatic Pattern: _String
Instrument
The instrument scans the potential (within a practical range) applied between the WorkingElectrode and the CounterElectrode inserted in the LoadingSample solution, and measures the potential difference between the WorkingElectrode and the ReferenceElectrode, and therefore performs the cyclic voltammetry measurements.
Format: Single
Class: Link
Programmatic Pattern: _Link
ReactionVesselHolder
The part attached to the cyclic voltammetry instrument that fix and support the reaction vessel(s) stable during the measurements.
Format: Single
Class: Link
Programmatic Pattern: _Link
Analytes
For each member of SamplesIn, indicates the molecule whose cyclic voltammograms are measured.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Model[Molecule]
WorkingElectrode
The electrode whose potential is linearly and periodically swept to trigger the local reduction and oxidation of the target analyte (SamplesIn for solid inputs) during the cyclic voltammetry measurement.
Format: Single
Class: Link
Programmatic Pattern: _Link
CounterElectrode
The electrode inserted into the same LoadingSample solution as the WorkingElectrode to form a complete electrical circuit.
Format: Single
Class: Link
Programmatic Pattern: _Link
ReferenceElectrodes
For each member of SamplesIn, indicates the electrode whose potential stays constant during the cyclic voltammetry measurement, and therefore can be used as reference point for the WorkingElectrode.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
ElectrodeCap
The cap of the ReactionVessel, which holds the WorkingElectrode, ReferenceElectrode, and CounterElectrode, and conductively connects them to the Instrument.
Format: Single
Class: Link
Programmatic Pattern: _Link
ReactionVessels
For each member of SamplesIn, indicates the container used to hold the LoadingSample solution to be measured, which the WorkingElectrode, ReferenceElectrode, and CounterElectrode are inserted into.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Replicate Experiments
Template
The protocol whose option selections should be selected as the default options for this protocol.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Protocol][ProtocolsTemplated]
ProtocolsTemplated
Protocols which were generated using this protocol's options as a starting point for its option defaults.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Protocol][Template]
Sample Preparation
PreparatoryUnitOperations
A list of transfers, consolidations, aliquots, mixes and dilutions that will be performed in the order listed to prepare samples for the experiment.
Format: Multiple
Class: Expression
Programmatic Pattern: _ | _
PreparatoryPrimitives
A list of transfers, consolidations, aliquots, mixes and dilutions that will be performed in the order listed to prepare samples for the experiment.
Format: Multiple
Class: Expression
Programmatic Pattern: _ | _
VolumeCheckSamplePrep
Indicates if any liquid samples prepared by using the PreparatoryUnitOperations option should have their volumes measured and updated before running the experiment.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
IncubateSamplePreparation
For each member of SamplesIn, parameters describing how the input samples should be heated prior to any aliquoting or the start of the experiment.
Format: Multiple
[Incubate]
Header: Incubate
Class: Boolean
[IncubationTemperature]
Header: IncubationTemperature
Class: Real
Unit: 1 degree Celsius
[IncubationTime]
Header: IncubationTime
Class: Real
Unit: 1 second
[Mix]
Header: Mix
Class: Boolean
[MixType]
Header: MixType
Class: Expression
[MixUntilDissolved]
Header: MixUntilDissolved
Class: Boolean
[MaxIncubationTime]
Header: MaxIncubationTime
Class: Real
Unit: 1 second
[IncubationInstrument]
Header: IncubationInstrument
Class: Link
[AnnealingTime]
Header: AnnealingTime
Class: Real
Unit: 1 second
[IncubateAliquotContainer]
Header: IncubateAliquotContainer
Class: Expression
[IncubateAliquot]
Header: IncubateAliquot
Class: Real
Unit: 1 liter
[IncubateAliquotDestinationWell]
Header: IncubateAliquotDestinationWell
Class: Expression
CentrifugeSamplePreparation
For each member of SamplesIn, parameters describing how the input samples should be spun down prior to any aliquoting or the start of the experiment.
Format: Multiple
[Centrifuge]
Header: Centrifuge
Class: Boolean
[CentrifugeInstrument]
Header: CentrifugeInstrument
Class: Link
[CentrifugeIntensity]
Header: CentrifugeIntensity
Class: VariableUnit
[CentrifugeTime]
Header: CentrifugeTime
Class: Real
Unit: 1 minute
[CentrifugeTemperature]
Header: CentrifugeTemperature
Class: Real
Unit: 1 degree Celsius
[CentrifugeAliquotContainer]
Header: CentrifugeAliquotContainer
Class: Expression
[CentrifugeAliquot]
Header: CentrifugeAliquot
Class: Real
Unit: 1 liter
[CentrifugeAliquotDestinationWell]
Header: CentrifugeAliquotDestinationWell
Class: Expression
FilterSamplePreparation
For each member of SamplesIn, parameters describing how particulates should be separated from the input samples prior to any aliquoting or the start of the experiment.
Format: Multiple
[Filtration]
Header: Filtration
Class: Boolean
[FiltrationType]
Header: FiltrationType
Class: Expression
[Filter]
Header: Filter
Class: Link
Relation: Object[Container] | Model[Container] | Object[Sample] | Model[Sample] | Object[Item] | Model[Item]
[FilterMaterial]
Header: FilterMaterial
Class: Expression
[FilterPoreSize]
Header: FilterPoreSize
Class: Real
Unit: 1 micrometer
[FilterContainerOut]
Header: FilterContainerOut
Class: Expression
[FilterInstrument]
Header: FilterInstrument
Class: Link
Relation: Model[Instrument, FilterBlock] | Object[Instrument, FilterBlock] | Model[Instrument, PeristalticPump] | Object[Instrument, PeristalticPump] | Model[Instrument, VacuumPump] | Object[Instrument, VacuumPump] | Model[Instrument, Centrifuge] | Object[Instrument, Centrifuge] | Model[Instrument, SyringePump] | Object[Instrument, SyringePump]
[FilterSyringe]
Header: FilterSyringe
Class: Link
[FilterHousing]
Header: FilterHousing
Class: Link
[FilterIntensity]
Header: FilterIntensity
Class: VariableUnit
[FilterTime]
Header: FilterTime
Class: Real
Unit: 1 minute
[FilterTemperature]
Header: FilterTemperature
Class: Real
Unit: 1 degree Celsius
[FilterSterile]
Header: FilterSterile
Class: Boolean
[FilterAliquotContainer]
Header: FilterAliquotContainer
Class: Expression
[FilterAliquot]
Header: FilterAliquot
Class: Real
Unit: 1 liter
[PrefilterMaterial]
Header: PrefilterMaterial
Class: Expression
[PrefilterPoreSize]
Header: PrefilterPoreSize
Class: Real
Unit: 1 micrometer
[FilterAliquotDestinationWell]
Header: FilterAliquotDestinationWell
Class: Expression
SamplePreparationProtocols
Protocols used to mix, centrifuge, incubate, and filter the SamplesIn prior to starting the experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
PooledIncubateSample Preparation
For each member of PooledSamplesIn, parameters describing how the pooled samples should be incubated after aliquoting but prior to the start of the experiment.
Format: Multiple
[Incubate]
Header: Incubate
Class: Boolean
[IncubationTemperature]
Header: IncubationTemperature
Class: Real
Unit: 1 degree Celsius
[IncubationTime]
Header: IncubationTime
Class: Real
Unit: 1 second
[Mix]
Header: Mix
Class: Boolean
[MixType]
Header: MixType
Class: Expression
[MixUntilDissolved]
Header: MixUntilDissolved
Class: Boolean
[MaxIncubationTime]
Header: MaxIncubationTime
Class: Real
Unit: 1 second
[IncubationInstrument]
Header: IncubationInstrument
Class: Link
[AnnealingTime]
Header: AnnealingTime
Class: Real
Unit: 1 second
[IncubateAliquotContainer]
Header: IncubateAliquotContainer
Class: Expression
[IncubateAliquot]
Header: IncubateAliquot
Class: Real
Unit: 1 liter
[IncubateAliquotDestinationWell]
Header: IncubateAliquotDestinationWell
Class: Expression
NestedIndexMatchingIncubate SamplePreparation
For each member of NestedIndexMatchingSamplesIn, parameters describing how the pooled samples should be incubated after aliquoting but prior to the start of the experiment.
Format: Multiple
[Incubate]
Header: Incubate
Class: Boolean
[IncubationTemperature]
Header: IncubationTemperature
Class: Real
Unit: 1 degree Celsius
[IncubationTime]
Header: IncubationTime
Class: Real
Unit: 1 second
[Mix]
Header: Mix
Class: Boolean
[MixType]
Header: MixType
Class: Expression
[MixUntilDissolved]
Header: MixUntilDissolved
Class: Boolean
[MaxIncubationTime]
Header: MaxIncubationTime
Class: Real
Unit: 1 second
[IncubationInstrument]
Header: IncubationInstrument
Class: Link
[AnnealingTime]
Header: AnnealingTime
Class: Real
Unit: 1 second
[IncubateAliquotContainer]
Header: IncubateAliquotContainer
Class: Expression
[IncubateAliquot]
Header: IncubateAliquot
Class: Real
Unit: 1 liter
[IncubateAliquotDestinationWell]
Header: IncubateAliquotDestinationWell
Class: Expression
PooledCentrifugeSample Preparation
For each member of PooledSamplesIn, parameters describing how the pooled samples should be centrifuge after aliquoting and pooled mixing but prior to the start of the experiment.
Format: Multiple
[Centrifuge]
Header: Centrifuge
Class: Boolean
[CentrifugeInstrument]
Header: CentrifugeInstrument
Class: Link
[CentrifugeIntensity]
Header: CentrifugeIntensity
Class: VariableUnit
[CentrifugeTime]
Header: CentrifugeTime
Class: Real
Unit: 1 minute
[CentrifugeTemperature]
Header: CentrifugeTemperature
Class: Real
Unit: 1 degree Celsius
[CentrifugeAliquotContainer]
Header: CentrifugeAliquotContainer
Class: Expression
[CentrifugeAliquot]
Header: CentrifugeAliquot
Class: Real
Unit: 1 liter
[CentrifugeAliquotDestinationWell]
Header: CentrifugeAliquotDestinationWell
Class: Expression
NestedIndexMatchingCentrifuge SamplePreparation
For each member of PooledSamplesIn, parameters describing how the pooled samples should be centrifuge after aliquoting and pooled mixing but prior to the start of the experiment.
Format: Multiple
[Centrifuge]
Header: Centrifuge
Class: Boolean
[CentrifugeInstrument]
Header: CentrifugeInstrument
Class: Link
[CentrifugeIntensity]
Header: CentrifugeIntensity
Class: VariableUnit
[CentrifugeTime]
Header: CentrifugeTime
Class: Real
Unit: 1 minute
[CentrifugeTemperature]
Header: CentrifugeTemperature
Class: Real
Unit: 1 degree Celsius
[CentrifugeAliquotContainer]
Header: CentrifugeAliquotContainer
Class: Expression
[CentrifugeAliquot]
Header: CentrifugeAliquot
Class: Real
Unit: 1 liter
[CentrifugeAliquotDestinationWell]
Header: CentrifugeAliquotDestinationWell
Class: Expression
FilteredSamples
Samples corresponding to filtered eluents of SamplesIn generated during sample preparation and intended for use in this experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Sample]
SampleDilutions
For each member of SamplesIn, indicates if the current SamplesIn is not fully prepared and further sample preparation steps are performed to generate the LoadingSample solution, which contains a Solvent, an Electrolyte, the SamplesIn, and an optional InternalStandard.
Format: Multiple
Class: Boolean
Programmatic Pattern: BooleanP
SolidSampleAmounts
For each member of SamplesIn, the mass amount of solid SamplesIn used to prepare the LoadingSample solution.
Format: Multiple
Class: Real
Unit: 1 milligram
Programmatic Pattern: GreaterP[0 Milligram]
LoadingSampleTarget Concentrations
For each member of SamplesIn, the concentration of SamplesIn in the prepared LoadingSample solution.
Format: Multiple
Class: VariableUnit
Programmatic Pattern: Milligram
Hold[GreaterP[0 Millimolar] | GreaterP[0 ----------]]
Milliliter
Solvents
For each member of SamplesIn, indicates the solvent sample identified from prepared liquid SamplesIn, or the solvent sample used to dissolve the solid SamplesIn, Electrolyte, and the optional InternalStandard to prepare the LoadingSample solution.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
RequestedSolvents
Indicates the solvent sample requested to dissolve the solid SamplesIn, Electrolyte, and the optional InternalStandard to prepare the LoadingSample solution.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
SolventVolumes
For each member of SamplesIn, indicates the volume of solvent used to prepare the LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: GreaterP[0 Milliliter]
Electrolytes
For each member of SamplesIn, indicates the chemical to be dissolved into the Solvent solution along with the solid SamplesIn and optional InternalStandard to prepare the LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
RequestedElectrolytes
Indicates the electrolyte sample requested to be dissolved with the solid SamplesIn and the optional InternalStandard within the Solvent to prepare the LoadingSample solution.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
LoadingSampleElectrolyte Amounts
For each member of SamplesIn, the mass amount of electrolyte used to prepare the LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: Real
Unit: 1 milligram
Programmatic Pattern: GreaterP[0 Milligram]
ElectrolyteTarget Concentrations
For each member of SamplesIn, the concentration of the electrolyte in the prepared LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: VariableUnit
Programmatic Pattern: Milligram
Hold[GreaterP[0 Millimolar] | GreaterP[0 ----------]]
Milliliter
InternalStandards
For each member of SamplesIn, indicates the chemical used as a potential reference point and being dissolved in the same Pretreatment solution as the SamplesIn to prepare the LoadingSample solution, if the InternalStandardAdditionOrder if Before. If the InternalStandardAdditionOrder is After, the InternalStandard is added into the LoadingSample solution after the cyclic voltammetry measurements, In this case, the LoadingSample solution added with InternalStandard is measured again with the same potential parameters specified in Primary/Secondary/Tertiary/Quaternary-CyclicVoltammetryPotentials.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
RequestedInternalStandards
Indicates the internal standard sample requested to be dissolved with the solid SamplesIn and the Electrolyte to within the Solvent prepare the LoadingSample solution.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
InternalStandardAddition Orders
For each member of SamplesIn, indicates the InternalStandard is added into LoadingSample solution before or after the cyclic voltammetry measurements. If the InternalStandardAdditionOrder is After, the LoadingSample solution added with InternalStandard is measured again with the same potential parameters specified in Primary/Secondary/Tertiary/Quaternary-CyclicVoltammetryPotentials.
Format: Multiple
Class: Expression
Programmatic Pattern: Before | After
InternalStandardAmounts
For each member of SamplesIn, if InternalStandardAdditionOrder is Before for an unprepared solid SamplesIn, indicates the mass amount of InternalStandard added into LoadingSample solution during the LoadingSample preparation process. If InternalStandardAdditionOrder is Before for a prepared liquid SamplesIn, InternalStandardAmount is Null and please refer to SamplesIn for InternalStandard information.
If the InternalStandardAdditionOrder is After, the LoadingSample solution is added with this amount of InternalStandard and is measured again with the same potential parameters specified in Primary/Secondary/Tertiary/Quaternary-CyclicVoltammetryPotentials.
Format: Multiple
Class: Real
Unit: 1 milligram
Programmatic Pattern: GreaterP[0 Milligram]
InternalStandardTarget Concentrations
For each member of SamplesIn, if InternalStandardAdditionOrder is Before for an unprepared solid SamplesIn, indicates the target concentration of InternalStandard added into LoadingSample solution during the LoadingSample preparation process. If InternalStandardAdditionOrder is Before for a prepared liquid SamplesIn, InternalStandardTargetConcentration is Null and please refer to SamplesIn for InternalStandard information.
If the InternalStandardAdditionOrder is After, the LoadingSample solution is added with InternalStandard to match the InternalStandardTargetConcentration and is measured again with the same potential parameters specified in Primary/Secondary/Tertiary/Quaternary-CyclicVoltammetryPotentials.
Format: Multiple
Class: VariableUnit
Programmatic Pattern: Milligram
Hold[GreaterP[0 Millimolar] | GreaterP[0 ----------]]
Milliliter
LoadingSamplePreparation Containers
For each member of SamplesIn, indicates the container used to perform the preparation of LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
LoadingSampleMixes
For each member of SamplesIn, indicates if the solution is mixed after the addition of the analyte, the electrolyte (if added) and the optional internal standard (addition order is before) into the solvent.
Format: Multiple
Class: Expression
Programmatic Pattern: BooleanP
LoadingSampleMixTypes
For each member of SamplesIn, indicates the mixing method to prepare the LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: Expression
Programmatic Pattern: Shake | Pipette | Invert
LoadingSampleMixTemperatures
For each member of SamplesIn, indicates the temperature at which the LoadingSample solution from solid SamplesIn is mixed.
Format: Multiple
Class: Real
Unit: 1 degree Celsius
Programmatic Pattern: RangeP[25 Celsius, 75 Celsius]
LoadingSampleMixTimes
For each member of SamplesIn, indicates the duration that the LoadingSample solution from solid SamplesIn is mixed.
Format: Multiple
Class: Real
Unit: 1 minute
Programmatic Pattern: GreaterP[0 Minute]
LoadingSampleNumberOfMixes
For each member of SamplesIn, indicates the number of mixes to prepare the LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: Integer
Programmatic Pattern: RangeP[0, 50, 1]
LoadingSampleMixVolumes
For each member of SamplesIn, indicates the solution volume that is pipetted up and down (if the MixType is Pipette) to prepare the LoadingSample solution from solid SamplesIn.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: RangeP[1 Milliliter, 20 Milliliter]
LoadingSampleMixUntil Dissolveds
For each member of SamplesIn, indicates if the mixing of the LoadingSample solution continues until the solid sample is dissolved, up to the LoadingSampleMaxMixTime or the LoadingSampleMaxNumberOfMixes.
Format: Multiple
Class: Expression
Programmatic Pattern: BooleanP
LoadingSampleMaxNumberOfMixes
For each member of SamplesIn, indicates the maximum number of mixes to prepare the LoadingSample solution from solid SamplesIn, in attempt to dissolve all the solids.
Format: Multiple
Class: Integer
Programmatic Pattern: RangeP[0, 50, 1]
LoadingSampleMaxMixTimes
For each member of SamplesIn, indicates the maximum duration of mixing to prepare the LoadingSample solution from solid SamplesIn, in attempt to dissolve all the solids.
Format: Multiple
Class: Real
Unit: 1 minute
Programmatic Pattern: GreaterP[0 Minute]
LoadingSamplePreparation Primitives
Instructions specifying the preparation of LoadingSamples solutions. First the Electrolyte is dissolved into the Solvent solution to prepare the ElectrolyteSolution. The ElectrolyteSolution is then used to mix the ReferenceCouplingSample to prepare the ReferenceSolution. The ElectrolyteSolution is also used to mix the solid SamplesIn and an optional InternalStandard to prepare the LoadingSample solution.
Format: Multiple
Class: Expression
Programmatic Pattern: SampleManipulationP
LoadingSamplePreparation Manipulations
The specific subprotocol to prepare the LoadingSamples solutions. First the Electrolyte is dissolved into the Solvent solution to prepare the ElectrolyteSolution. The ElectrolyteSolution is then used to mix the ReferenceCouplingSample to prepare the ReferenceSolution. The ElectrolyteSolution is also used to mix the solid SamplesIn and an optional InternalStandard to prepare the LoadingSample solution.
Format: Single
Class: Link
Programmatic Pattern: _Link
Relation: Object[Protocol]
LoadingSamples
For each member of SamplesIn, indicates the prepared solution including the solid SamplesIn, an Electrolyte, an optional InternalStandard dissolved in the Solvent solution. The LoadingSample solution is loaded into the ReactionVessel and measured by the cyclic voltammetry cycles.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Aliquoting
AliquotSamplePreparation
For each member of AliquotSamples, parameters describing how aliquots should be drawn from the input samples after initial sample preparation in order to create new aliquot samples upon which aliquot preparation and the experiment should proceed.
Format: Multiple
[Aliquot]
Header: Aliquot
Class: Boolean
[AliquotAmount]
Header: AliquotAmount
Class: Expression
[TargetConcentration]
Header: TargetConcentration
Class: Expression
[AssayVolume]
Header: AssayVolume
Class: Real
Unit: 1 milliliter
[AliquotContainer]
Header: AliquotContainer
Class: Expression
[AssayBuffer]
Header: AssayBuffer
Class: Link
[BufferDiluent]
Header: BufferDiluent
Class: Link
[BufferDilutionFactor]
Header: BufferDilutionFactor
Class: Real
[ConcentratedBuffer]
Header: ConcentratedBuffer
Class: Link
[DestinationWell]
Header: DestinationWell
Class: Expression
[TargetConcentrationAnalyte]
Header: TargetConcentrationAnalyte
Class: Expression
[AliquotSampleLabel]
Header: AliquotSampleLabel
Class: String
AliquotProtocols
Protocols used to create AliquotSamples prior to starting the experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Protocol]
AliquotPreparationProtocols
Protocols used to mix, centrifuge, incubate, and filter the AliquotSamples prior to starting the experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Protocol]
AliquotSamples
Samples corresponding to aliquots of SamplesIn generated during sample preparation and intended for use in this experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Sample]
AliquotContainers
Containers that hold AliquotSamples generated during sample preparation and intended for use in this experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
SaveAliquots
Indicates if the AliquotSamples should be stored after the experiment, rather than being discarded.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
ConsolidateAliquots
Indicates if identical aliquots should be consolidated in a single sample.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
AliquotPreparation
Indicates if the aliquotting should occur manually or on a robotic liquid handler.
Format: Single
Class: Expression
Programmatic Pattern: PreparationMethodP
AliquotVolumes
For each member of SamplesIn, the volume transferred from the sample into the aliquot sample which is used in lieu of the initial sample for the experiment.
Format: Multiple
Class: Real
Unit: 1 microliter
Programmatic Pattern: GreaterP[0 Micro Liter]
AliquotMasses
For each member of SamplesIn, the mass of a solid transferred from the sample into the aliquot sample which is used in lieu of the initial sample for the experiment.
Format: Multiple
Class: Real
Unit: 1 milligram
Programmatic Pattern: GreaterP[0 Milligram]
AliquotAmounts
For each member of SamplesIn, the amount transferred from the sample into the aliquot sample which is used in lieu of the initial sample for the experiment.
Format: Multiple
Class: VariableUnit
Programmatic Pattern: GreaterP[0 Milliliter] | GreaterP[0 Milligram] | GreaterP[0 Unit, 1 Unit]
TargetConcentrations
For each member of SamplesIn, the final concentration of analyte in the aliquot sample which is used in lieu of the initial sample for the experiment.
Format: Multiple
Class: Expression
Programmatic Pattern: Milligram
Hold[GreaterP[0 Micro Molar] | GreaterP[0 ----------]]
Milliliter
AssayVolumes
For each member of SamplesIn (or PooledSamplesIn), the total volume of the reaction mixture which is used in lieu of the initial sample for the experiment.
Format: Multiple
Class: Real
Unit: 1 microliter
Programmatic Pattern: GreaterEqualP[0 Micro Liter]
AssayBuffers
For each member of SamplesIn (or PooledSamplesIn), the final buffers used to generate AliquotSamples by aliquoting SamplesIn.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
ConcentratedBuffers
For each member of SamplesIn (or PooledSamplesIn), the concentrated buffer source which is added to the AliquotSamples to obtain 1x buffer concentration after dilution of the AliquotSamples which are used in lieu of the SamplesIn for the experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
BufferDilutionFactors
For each member of SamplesIn (or PooledSamplesIn), he dilution factor by which the concentrated buffer is diluted in preparing the AliquotSamples to obtain a 1x buffer concentration after dilution of the AliquotSamples which are used in lieu of the SamplesIn for the experiment.
Format: Multiple
Class: Real
Programmatic Pattern: GreaterP[0]
BufferDiluents
For each member of SamplesIn (or PooledSamplesIn), the diluent used to dilute the concentration of the concentrated buffer in preparing the AliquotSamples which are used in lieu of the SamplesIn for the experiment.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
ConcentratedBuffer
The concentrated buffer source which is added to each of the AliquotSamples to obtain 1x buffer concentration after dilution of the AliquotSamples which are used in lieu of the SamplesIn for the experiment.
Format: Single
Class: Link
Programmatic Pattern: _Link
BufferDilutionFactor
The dilution factor by which the concentrated buffer is diluted in preparing the AliquotSamples to obtain a 1x buffer concentration after dilution of the AliquotSamples which are used in lieu of the SamplesIn for the experiment.
Format: Single
Class: Integer
Programmatic Pattern: GreaterP[0]
BufferDiluent
The diluent used to dilute the concentration of the concentrated buffer in preparing the AliquotSamples which are used in lieu of the SamplesIn for the experiment.
Format: Single
Class: Link
Programmatic Pattern: _Link
AssayBuffer
The desired buffer for the AliquotSamples which are used in lieu of the SamplesIn for the experiment.
Format: Single
Class: Link
Programmatic Pattern: _Link
Sample Post-Processing
PostProcessingProtocols
Protocols used to perform post-processing such as sample imaging or volume measurement.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Protocol]
ImageSample
Indicates if the samples that are modified in the course of the experiment are imaged after running the experiment.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
MeasureVolume
Indicates if the volume of the liquid samples modified in the course of the experiment are measured after running the experiment.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
MeasureWeight
Indicates if the weight of the solid samples modified in the course of the experiment are measured after running the experiment.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
Measure
Indicates if the volume/weight of the samples modified in the course of the experiment are measured after running the experiment.
Format: Single
Class: Expression
Programmatic Pattern: BooleanP
Storage
Indicates the conditions under which any samples generated by this experiment are stored after the protocol is completed.
Format: Single
Class: Expression
Programmatic Pattern: SampleStorageTypeP | Disposal
Experimental Results
Data
Any primary data generated by this protocol.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
SamplesOut
Any preparative samples generated by the protocol.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
ContainersOut
Any containers holding SamplesOut generated by this protocol.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
EnvironmentalData
Measurements of environmental conditions (temperature and humidity) recorded during the execution of this protocol.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
LoadingSampleVolumes
For each member of SamplesIn, indicates the volume of prepared LoadingSample solution loaded into the ReactionVessel before the cyclic voltammetry measurements.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: GreaterP[0 Milliliter]
PrimaryCyclicVoltammetry Potentials
For each member of SamplesIn, indicates the potential (voltage) details of the first cyclic voltammetry measurement, which starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
SecondaryCyclicVoltammetry Potentials
For each member of SamplesIn, indicates the potential (voltage) details of the second cyclic voltammetry measurement, which starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
TertiaryCyclicVoltammetry Potentials
For each member of SamplesIn, indicates the potential (voltage) details of the third cyclic voltammetry measurement, which starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
QuaternaryCyclicVoltammetry Potentials
For each member of SamplesIn, indicates the potential (voltage) details of the fourth cyclic voltammetry measurement, which starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
NumberOfCycles
For each member of SamplesIn, indicates the number of cyclic voltammetry measurement cycles performed. A cyclic voltammetry measurement cycle starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by the SweepRate.
Format: Multiple
Class: Integer
Programmatic Pattern: RangeP[1, 4, 1]
CyclicVoltammetryData
For each member of SamplesIn, indicates the data object containing the cyclic voltammetry measurement results. The measurements are performed using the parameters specified in Primary/Secondary/Tertiary/Quaternary-CyclicVoltammetryPotentials.
Format: Multiple
Class: Link
Programmatic Pattern: Link
Relation: Object[Data][Protocol]
InitialLoadingSample Appearances
The image of the LoadingSample solution within the reaction vessel taken immediately before the cyclic voltammetry measurements.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[EmeraldCloudFile]
FinalLoadingSampleAppearances
The image of the LoadingSample solution within the reaction vessel taken immediately after the cyclic voltammetry measurements.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[EmeraldCloudFile]
PostMeasurementStandard AdditionData
For each member of SamplesIn, indicates the data object containing the cyclic voltammetry measurement results after the addition of InternalStandard into the LoadingSamples. The measurements are performed with the same parameters specified in Primary/Secondary/Tertiary/Quaternary-CyclicVoltammetryPotentials.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
InitialPostMeasurement StandardAdditionSample Appearances
The image of the PostMeasurementStandardAdditionSamples solution within the reaction vessel taken immediately before the cyclic voltammetry measurements.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[EmeraldCloudFile]
FinalPostMeasurementStandard AdditionSampleAppearances
The image of the PostMeasurementStandardAdditionSamples solution within the reaction vessel taken immediately after the cyclic voltammetry measurements.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[EmeraldCloudFile]
Troubleshooting
TroubleshootingReports
Reports for errors that require troubleshooting associated with the execution of this top-level protocol.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Resources
AwaitingResources
Indicates if this protocol is awaiting the arrival of items before it can be begun or continued.
Format: Single
Class: Boolean
Programmatic Pattern: BooleanP
ShippingMaterials
Indicates the transactions, and the specific products or samples therein, that must be received before this protocol can be begun or continued.
Format: Multiple
[[1]] Transaction
Header: Transaction
Class: Link
Programmatic Pattern: _Link
[[2]] Required Product
Header: Required Product
Class: Link
Programmatic Pattern: _Link
HazardousWaste
The types of waste generated by this protocol.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
DispenserContainers
Containers gathered as destinations for any resources obtained from a chemical dispenser.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
GasSources
A list of containers that supplied gas to instruments in this protocol through plumbing connections.
Format: Multiple
[[1]] Gas Type
Header: Gas Type
Class: Expression
Programmatic Pattern: GasP
[[2]] Source Container
Header: Source Container
Class: Link
Programmatic Pattern: _Link
Relation: Object[Container]
[[3]] Supplied Instrument
Header: Supplied Instrument
Class: Link
Programmatic Pattern: _Link
Relation: Object[Instrument]
Cleaning
WasteGenerated
For each type of waste generated by this protocol, the total amount (in grams) generated during the conduct of the protocol.
Format: Multiple
[Waste]
Header: Waste
Class: Link
Relation: Model[Sample]
[Weight]
Header: Weight
Class: Real
Unit: 1 gram
Storage Information
StoragePrice
The total monthly price for warehousing all user owned items associated with this protocol in an ECL facility under the storage conditions specified by each item.
Format: Single
Class: Real
Unit: 1 US dollar per month
Programmatic Pattern: USD
Hold[GreaterEqualP[0 -----]]
Month
Sample Storage
SamplesInStorage
For each member of SamplesIn, The storage conditions under which any input samples to this experiment should be stored after their usage in this experiment.
Format: Multiple
Class: Expression
Programmatic Pattern: SampleStorageTypeP | Disposal
AliquotStorage
For each member of AliquotSamples, The storage conditions under which any aliquot samples generated by this experiment should be stored after the protocol is completed.
Format: Multiple
Class: Expression
Programmatic Pattern: SampleStorageTypeP | Disposal
SamplesOutStorage
For each member of SamplesOut, the storage conditions under which any output samples generated by this experiment should be stored after the protocol is completed.
Format: Multiple
Class: Expression
Programmatic Pattern: SampleStorageTypeP | Disposal
Option Handling
ResolvedOptions
The final options used as parameters for this protocol, after automatic options are resolved.
Format: Single
Class: Compressed
Programmatic Pattern: {_Rule...}
UnresolvedOptions
The verbatim options originally input by the protocol author to generate this protocol, often with some options set to Automatic.
Format: Single
Class: Compressed
Programmatic Pattern: {_Rule...}
Computations
ParallelComputations
List of computational jobs generated and run in parallel to the execution of this protocol.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
ComputationsOutstanding
Indicates if any of the computation jobs in ParallelComputations have not yet completed.
Format: Single
Class: Boolean
Programmatic Pattern: BooleanP
ErroneousComputations
List of computational jobs generated and run in parallel to the execution of this protocol in which a warning or error was thown, or that did not finish.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Electrode Polishing
PrimaryPolishings
For each member of SamplesIn, indicates the polishing pad, polishing solution, the number of polishing solution droplets added onto the polishing pad, and the number of polishings for the first polishing in the working electrode polishing process.
Format: Multiple
[PolishingPad]
Header: PolishingPad
Class: Link
[PolishingSolution]
Header: PolishingSolution
Class: Link
[PolishingPlate]
Header: PolishingPlate
Class: Link
[NumberOfDroplets]
Header: NumberOfDroplets
Class: Integer
[NumberOfPolishings]
Header: NumberOfPolishings
Class: Integer
SecondaryPolishings
For each member of SamplesIn, indicates the polishing pad, polishing solution, the number of polishing solution droplets added onto the polishing pad, and the number of polishings for the second polishing in the working electrode polishing process.
Format: Multiple
[PolishingPad]
Header: PolishingPad
Class: Link
[PolishingSolution]
Header: PolishingSolution
Class: Link
[PolishingPlate]
Header: PolishingPlate
Class: Link
[NumberOfDroplets]
Header: NumberOfDroplets
Class: Integer
[NumberOfPolishings]
Header: NumberOfPolishings
Class: Integer
TertiaryPolishings
For each member of SamplesIn, indicates the polishing pad, polishing solution, the number of polishing solution droplets added onto the polishing pad, and the number of polishings for the third polishing in the working electrode polishing process.
Format: Multiple
[PolishingPad]
Header: PolishingPad
Class: Link
[PolishingSolution]
Header: PolishingSolution
Class: Link
[PolishingPlate]
Header: PolishingPlate
Class: Link
[NumberOfDroplets]
Header: NumberOfDroplets
Class: Integer
[NumberOfPolishings]
Header: NumberOfPolishings
Class: Integer
WorkingElectrodePolishWashing Solutions
For each member of SamplesIn, indicates if the solutions used to wash the working electrode after the working electrode is polished. The washing process includes "Milli-Q" water and methanol squirted from a wash bottle against the electrode in sequence. For the working electrode, a chemwipe damped with the methanol is used to carefully wipe its bottom surface. The electrode is blow dried with nitrogen gas at the end.
Format: Multiple
[Primary]
Header: Primary
Class: Link
[Secondary]
Header: Secondary
Class: Link
UniquePolishingSolutions
Indicates the unique polishing solutions used during the working electrode polishing process.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
UniquePolishingSolution Volumes
For each member of UniquePolishingSolutions, indicates the volume required by this protocol.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: GreaterP[0 Milliliter]
UniquePolishingPads
Indicates the unique polishing pads used during the working electrode polishing process.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
UniquePolishingPlates
For each member of UniquePolishingPads, indicates the plate used to support the polishing pad during the working electrode polishing process.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Electrode Cleaning
WorkingElectrodeSonication Times
For each member of SamplesIn, indicates the duration for each working electrode sonication process. If the current sonication time is 0 second, the sonication process is skipped.
Format: Multiple
Class: Real
Unit: 1 second
Programmatic Pattern: GreaterP[0 Second]
WorkingElectrodeSonication Temperatures
For each member of SamplesIn, indicates the sonication bath temperature for each working electrode sonication process.
Format: Multiple
Class: Real
Unit: 1 degree Celsius
Programmatic Pattern: GreaterP[0 Kelvin]
WorkingElectrodeWashing Solutions
For each member of SamplesIn, indicates if the working electrode washing is performed. An electrode washing process includes "Milli-Q" water and methanol squirted from a wash bottle against the electrode in sequence. For the working electrode, a Chemwipe damped with the methanol is used to carefully wipe its bottom surface. After the washing, the electrode is blow tap dried with a piece of Chemwipe.
Format: Multiple
[Primary]
Header: Primary
Class: Link
[Secondary]
Header: Secondary
Class: Link
CounterElectrodeWashing Solutions
For each member of SamplesIn, indicates if the counter electrode washing is performed. An electrode washing process includes "Milli-Q" water and methanol squirted from a wash bottle against the electrode in sequence. After the washing, the electrode is blow tap dried with a piece of Chemwipe.
Format: Multiple
[Primary]
Header: Primary
Class: Link
[Secondary]
Header: Secondary
Class: Link
WorkingElectrodeWashingCycles
For each member of SamplesIn, indicates the number of washing cycles performed in the working electrode washing process. A washing cycle includes going through all the washing solutions specified in the WorkingElectrodeWashingSolutions option.
Format: Multiple
Class: Integer
Programmatic Pattern: RangeP[0, 10, 1]
UniqueElectrodeWashing Solutions
Unique washing solution samples to wash the working-, counter-, reference electrodes.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
UniqueElectrodeWashing SolutionVolumes
For each member of UniqueElectrodeWashingSolutions, the volume used during this protocol.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: GreaterP[0 Milliliter]
WashingSolutionsCollection Containers
For each member of UniqueElectrodeWashingSolutions, the temporary container collects the electrode washing solution before the used solution is transferred into the waste container.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Reference Electrode Preparation
RefreshReferenceElectrodes
For each member of SamplesIn, indicates if the ReferenceElectrode is refreshed using the ReferenceSolution defined in the ReferenceElectrode.
Format: Multiple
Class: Expression
Programmatic Pattern: BooleanP
ReferenceElectrodeSoakTimes
For each member of SamplesIn, the duration for which the soaking of the ReferenceElectrode within the ElectrolyteSolution or LoadingSample solution lasts.
Format: Multiple
Class: Real
Unit: 1 minute
Programmatic Pattern: GreaterP[0 Minute]
Electrode Pretreatment
ElectrolyteSolutions
For each member of SamplesIn, indicates the solution that contains a Solvent and an Electrolyte to be used during the electrodes pretreatment process.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
ElectrolyteSolutionLoading Volumes
For each member of SamplesIn, indicates the loading volume of the ElectrolyteSolution into the ReactionVessel.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: GreaterP[0 Milliliter]
PretreatmentReactionVessels
For each member of SamplesIn, indicates the container used to hold the ElectrolyteSolution for the electrode pretreatment process.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
PretreatmentSpargingGases
For each member of SamplesIn, indicates the type of inert gas used for the sparging process before the cyclic voltammetry measurement.
Format: Multiple
Class: Expression
Programmatic Pattern: InertGasP
PretreatmentSpargingTimes
For each member of SamplesIn, indicates the duration of the inert gas sparging of the ElectrolyteSolution for the electrode pretreatment process.
Format: Multiple
Class: Real
Unit: 1 minute
Programmatic Pattern: GreaterP[0 Minute]
PretreatmentSpargingPressures
For each member of SamplesIn, indicates the inert gas sparging pressure of the ElectrolyteSolution for the electrode pretreatment process.
Format: Multiple
Class: Real
Unit: 1 pound‐force per inch squared
Programmatic Pattern: GreaterP[0 PSI]
PretreatmentSpargingPressure Logs
The pressure logs for the pretreatment sparging gas source for each SamplesIn.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
PretreatmentSpargingPre Bubblers
For each member of SamplesIn, indicates if a prebubbler is used before the electrode pretreatment reaction vessel. A prebubbler is a container containing the same Solvent used to prepare the LoadingSample, which is hooked in series with the reaction vessel, such that the gas is first bubbled through the prebubbler solution and then bubbled into the reaction vessel. This helps to ensure the reaction vessel doesn't excessively evaporate during the sparging, since the sparging gas is saturated by the solvent inside the prebubbler before travelling into the reaction vessel.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
PretreatmentSpargingPre BubblerSolvents
For each member of SamplesIn, indicates the solvent sample loaded into the PreBubbler for ElectrolyteSolution sparging before the ElectrolyteSolution is used for the electrodes pretreatment process.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
PretreatmentSpargingPre BubblerSolventVolumes
For each member of SamplesIn, indicates the volume of Solvent is loaded into the PreBubbler for ElectrolyteSolution sparging before the ElectrolyteSolution is used for the electrodes pretreatment process.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: GreaterP[0 Milliliter]
PretreatmentPrimaryPotentials
For each member of SamplesIn, indicates the electrode pretreatment potential details of the first pretreatment cycle. A pretreatment cycle starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
PretreatmentSecondary Potentials
For each member of SamplesIn, indicates the electrode pretreatment potential details of the second pretreatment cycle. A pretreatment cycle starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
PretreatmentTertiary Potentials
For each member of SamplesIn, indicates the electrode pretreatment potential details of the third pretreatment cycle. A pretreatment cycle starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
PretreatmentQuaternary Potentials
For each member of SamplesIn, indicates the electrode pretreatment potential details of the fourth pretreatment cycle. A pretreatment cycle starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
[InitialPotential]
Header: InitialPotential
Class: Real
Unit: 1 millivolt
[FirstPotential]
Header: FirstPotential
Class: Real
Unit: 1 millivolt
[SecondPotential]
Header: SecondPotential
Class: Real
Unit: 1 millivolt
[FinalPotential]
Header: FinalPotential
Class: Real
Unit: 1 millivolt
[SweepRate]
Header: SweepRate
Class: Real
Unit: 1 millivolt per second
PretreatmentNumberOfCycles
For each member of SamplesIn, indicates the number of electrode pretreatment cycle performed. A pretreatment cycle starts at the InitialPotential, then to FirstPotential, then to SecondPotential, and stops at the FinalPotential. During this process, the WorkingElectrode potential is linearly swept between these potential points with a speed specified by SweepRate.
Format: Multiple
Class: Integer
Programmatic Pattern: RangeP[0, 4, 1]
ElectrodePretreatmentData
For each member of SamplesIn, indicates the data object containing the cyclic voltammetry results obtained during the electrode pretreatment process. The measures are performed using the parameters specified by PretreatmentPrimaryPotentials, PretreatmentSecondaryPotentials, PretreatmentTertiaryPotentials, and PretreatmentQuaternaryPotentials.
Format: Multiple
Class: Link
Programmatic Pattern: Link
Relation: Object[Data][Protocol]
Sparging
SpargingGases
For each member of SamplesIn, indicates the type of inert gas used for the sparging process before the cyclic voltammetry measurement.
Format: Multiple
Class: Expression
Programmatic Pattern: InertGasP
SpargingTimes
For each member of SamplesIn, indicates the duration used for the sparging process before the cyclic voltammetry measurement.
Format: Multiple
Class: Real
Unit: 1 minute
Programmatic Pattern: GreaterP[0 Minute]
SpargingPressures
For each member of SamplesIn, indicates the inert gas sparging pressure before the cyclic voltammetry measurement.
Format: Multiple
Class: Real
Unit: 1 pound‐force per inch squared
Programmatic Pattern: GreaterP[0 PSI]
SpargingPressureLogs
The pressure logs for the sparging gas source for each SamplesIn.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
SpargingPreBubblers
For each member of SamplesIn, indicates the prebubbler used before the reaction vessel. A prebubbler is a container containing the same solvent used in the electrolyte solution, which is hooked in series with the reaction vessel, such that the gas is first bubbled through the prebubbler solution and then bubbled into the reaction vessel. This helps to ensure the reaction vessel doesn't excessively evaporate during the sparging, since the sparging gas is saturated by the solvent inside the prebubbler before travelling into the reaction vessel.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
SpargingPreBubblerSolvents
For each member of SamplesIn, indicates the solvent sample loaded into the PreBubbler for LoadingSample solution sparging before the LoadingSample is measured by cyclic voltammetry cycles.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
SpargingPreBubblerSolvent Volumes
For each member of SamplesIn, indicates the volume of solvent sample loaded into the PreBubbler for LoadingSample solution sparging before the LoadingSample is measured by cyclic voltammetry cycles.
Format: Multiple
Class: Real
Unit: 1 milliliter
Programmatic Pattern: GreaterP[0 Milliliter]
Post Measurement Internal Standard Addition
PostMeasurementStandard AdditionContainers
For each member of SamplesIn, the container for the addition and mixing of the internal standard after the cyclic voltammetry measurements.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
PostMeasurementStandard AdditionPrimitives
Accumulated instructions specifying the mix of InternalStand into the LoadingSamples solutions after the cyclic voltammetry measurements of the LoadingSamples.
Format: Multiple
Class: Expression
Programmatic Pattern: SamplePreparationP
PostMeasurementStandard AdditionManipulations
The subprotocols performed to mix the InternalStandard into the LoadingSamples solution after the cyclic voltammetry measurements of the LoadingSamples, but before the solution is measured again with the same parameters specified in Primary/Secondary/Tertiary/Quaternary-CyclicVoltammetryPotentials.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Protocol]
PostMeasurementStandard AdditionSamples
For each member of SamplesIn, if the InternalStandardAdditional order is After, the sample object after the InternalStandard is mixed into the LoadingSamples after the cyclic voltammetry measurements.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Sample]
PostMeasurementStandard AdditionSpargingPressureLogs
The pressure logs for the sparging gas source during the post measurement internal standard addition sparging process for each SamplesIn.
Format: Multiple
Class: Link
Programmatic Pattern: _Link
Relation: Object[Data][Protocol]
Last modified on Mon 26 Sep 2022 15:43:49